{"id":1448,"date":"2020-06-30T16:32:45","date_gmt":"2020-06-30T16:32:45","guid":{"rendered":"https:\/\/uni.hi.is\/tobi\/?page_id=1448"},"modified":"2020-07-10T07:11:29","modified_gmt":"2020-07-10T07:11:29","slug":"what-we-do-in-the-labs","status":"publish","type":"page","link":"https:\/\/uni.hi.is\/tobi\/what-we-do-in-the-labs\/","title":{"rendered":"What we do in the labs"},"content":{"rendered":"<h1>Melt fragmentation experiments<\/h1>\n<p>So, what has caused this abundance of ash during the 2012 Havre eruption? Let's draft a list of \"major suspects\", i.e. potential ash generation mechanisms that could have produced these fragments:<\/p>\n<ul>\n<li>Thermal granulation<\/li>\n<li>Magmatic fragmentation<\/li>\n<li>Fuel-coolant interaction<\/li>\n<\/ul>\n<p>Each of these mechanisms were reproduced in the lab in W\u00fcrzburg.<\/p>\n<p>We have <a href=\"https:\/\/uni.hi.is\/tobi\/fragmentation\/\">previously discussed<\/a> what affects the shape of fragments. Important controlling factors are [1]: pre-stresses (which affects the locals stress distribution); the existence of shock-waves; and how exactly the driving stress was generated. The latter factor can be basically broken down to the question:<\/p>\n<p>\"<strong>Which amount and what kind of energy was driving fragmentation?<\/strong>\"<\/p>\n<p>It is therefore usefult to discuss the \"energy question\" for each of the listed fragmentation mechanisms.<\/p>\n<h2>Thermal granulation by quenching<\/h2>\n<p>Imagine you have a drinking glass and heat it up to 230\u00b0C in a pizza oven. If<\/p>\n<p><div id=\"attachment_1449\" style=\"width: 221px\" class=\"wp-caption alignright\"><a href=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/2020-06-04-15_20_56-Mendeley-Desktop.jpg\"><img loading=\"lazy\" decoding=\"async\" aria-describedby=\"caption-attachment-1449\" class=\"wp-image-1449\" src=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/2020-06-04-15_20_56-Mendeley-Desktop.jpg\" alt=\"\" width=\"211\" height=\"367\" srcset=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/2020-06-04-15_20_56-Mendeley-Desktop.jpg 288w, https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/2020-06-04-15_20_56-Mendeley-Desktop-172x300.jpg 172w\" sizes=\"auto, (max-width: 211px) 100vw, 211px\" \/><\/a><p id=\"caption-attachment-1449\" class=\"wp-caption-text\">Thermal granulation experiment with a basaltic Gr\u00edmsv\u00f6tn melt at a temperature of 1300\u00b0C, poured into water. (Adapted from Schipper et al. (2013) [2])<\/p><\/div>you put it out and fill it with cold water, chances are high that the glass will crack and shatter. This process is called \"thermal granulation\", and it is the more efficient the larger the temperature contrast between hot melt and coolant is.<\/p>\n<p>&nbsp;<\/p>\n<p>When magmatic glassy melt is rapidly cooled by water, what happens is that immediately a crust is formed at the interface. With cooling the melt contracts, and the hotter (and more moveable) inner parts of the melt exert tensional stress on the colder (more rigid) crust. As described <a href=\"http:\/\/uni.hi.is\/tobi\/fragmentation\/\">in an earlier post<\/a>, mechanical stress is the fuel that drives the cracks - so no wonder, that qenching cracks are observed, when magma meets water.<\/p>\n<p>In the Physikalisch-Vulkanologisches Labor, Uni W\u00fcrzburg, thermal granulation was reproduced by remelting crushed Havre dome rock (as well as pumice), using an induction coil. Then the melt was extruded and plunged into a water tank.<\/p>\n<p>An alternative approach is to heat coarse ash or lapili to 500\u00b0C and pour the grains into a water container.<\/p>\n<div id=\"attachment_1450\" style=\"width: 255px\" class=\"wp-caption aligncenter\"><a href=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/Bismarck1.gif\"><img loading=\"lazy\" decoding=\"async\" aria-describedby=\"caption-attachment-1450\" class=\"wp-image-1450\" src=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/Bismarck1.gif\" alt=\"\" width=\"245\" height=\"211\" \/><\/a><p id=\"caption-attachment-1450\" class=\"wp-caption-text\">Thermal granulation experiments with lapilli sized dome rock grains. These particles were heated to 500\u00b0C before being poured into a calorimeter containing 3 l of water at room temperature.<\/p><\/div>\n<p>Now to the \"energy question\" - how is fracture energy provided in thermal granulation? Well, the stresses occur because of cooling. We can therefore link thermal granulation processes with the heat carried by the melt.<\/p>\n<h2>Abrasion<\/h2>\n<p>To mimic abrasion, pieces of pumice were \"scrubbed\" against each other over a piece of paper. Simple, but effective.<\/p>\n<p>And it is also simple to identify the energies \"responsible\" for producing these particles: the mechanical energy was provided by the person who grinded the pieces of pumice against another.<\/p>\n<h2>Magmatic fragmentation: \"dry\" stress-induced melt fragmentation experiments<\/h2>\n<p><div id=\"attachment_1480\" style=\"width: 325px\" class=\"wp-caption aligncenter\"><a href=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_setup.jpg\"><img loading=\"lazy\" decoding=\"async\" aria-describedby=\"caption-attachment-1480\" class=\"wp-image-1480\" src=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_setup.jpg\" alt=\"\" width=\"315\" height=\"229\" srcset=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_setup.jpg 600w, https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_setup-300x218.jpg 300w\" sizes=\"auto, (max-width: 315px) 100vw, 315px\" \/><\/a><p id=\"caption-attachment-1480\" class=\"wp-caption-text\">Experimental setup for \"dry\" stress-induced fragmentation runs. (Illustration adapted from D\u00fcrig et al. (2020) [3].)<\/p><\/div><a href=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry.gif\"><img loading=\"lazy\" decoding=\"async\" class=\"wp-image-1461 alignleft\" src=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry.gif\" alt=\"\" width=\"161\" height=\"174\" \/><\/a> \"Dry\" stress-induced melt fragmentation run routines are used to determine material-specific fragmentation and kinetic energy release rates [4]. In these experiments, pressurized argon is injected from below at high pressure into a cylindrical plug of melt that behaves brittlely when deformed by the expanding injected gas. When the critical shear stress is reached the plug breaks, with elastically stored energy converted into fragmentation and kinetic energy. The pressure of the driving gas is measured, and a force sensor under the crucible recorded recoil of the system.<\/p>\n<p>The following flow chart illustrates what happens in a \"dry\" stress-induced fragmentation run.<\/p>\n<p><a href=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_flow.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-1483\" src=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_flow-1024x888.jpg\" alt=\"\" width=\"337\" height=\"292\" srcset=\"https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_flow-1024x888.jpg 1024w, https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_flow-300x260.jpg 300w, https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_flow-768x666.jpg 768w, https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_flow-1536x1332.jpg 1536w, https:\/\/uni.hi.is\/tobi\/files\/2020\/06\/dry_flow.jpg 1748w\" sizes=\"auto, (max-width: 337px) 100vw, 337px\" \/><\/a>So which energy is causing the melt to fracture? It is purely mechanical work, applied by the expanding gas. (The use of gas has the great operational advantage that we can control its volume and pressure - and thus the input energy, which is simply the product of these two parameters [4].)<\/p>\n<p>The mechanical energy input is therefore provided by an <em>external<\/em> source and - and not by the melt. Importantly, the temperature of the melt does not (or at least not much) change during the few ten microseconds of fragmentation. Physicists would therefore call this type of fragmentation a \"<em>quasi-isothermal\" <\/em>stress-induced process.<\/p>\n<p>This is a crucial difference to fuel coolant interaction processes, which are discussed in the next post.<\/p>\n<p><a href=\"https:\/\/uni.hi.is\/tobi\/mfci-vs-ifci\/\">-&gt; Explosive Fuel Coolant-Interaction<\/a><\/p>\n<h3><span style=\"text-decoration: underline\">Annotations<\/span>:<\/h3>\n<p><em>The Havre ash project was funded by a Marsden grant, New Zealand.<\/em><\/p>\n<p><em>The lines of thought above are based on considerations detailed in D\u00fcrig et al. (2020) [3], if not cited otherwise. Please let me know if you have any comment or suggestions for changes. My email address is: tobi[_at]hi.is<\/em><\/p>\n<h2>References and Annotations<\/h2>\n<p>[1]: T. D\u00fcrig &amp; B. Zimanowski, \u201cBreaking news\u201d on the formation of volcanic ash: Fracture dynamics in silicate glass. <em>Earth and Planetary Science Letters<\/em> 335, 1-8 (2012)<\/p>\n<p>[2]: C. I. Schipper, I. Sonder, et al. Vapour dynamics during magma\u2013water interaction experiments: hydromagmatic origins of submarine volcaniclastic particles (limu o Pele). <em>Geophysical Journal International<\/em> 192 (3) 1109-1115<\/p>\n<p><a href=\"https:\/\/rdcu.be\/b5nVg\">[3]: T. D\u00fcrig, J.D.L. White, A.P. Murch, B. Zimanowski, R. B\u00fcttner, D. Mele, P. Dellino, R.J. Carey, L.S. Schmidt, N. Spitznagel, Deep-sea eruptions boosted by induced fuel-coolant explosions. <em>Nature Geoscience<\/em> <b data-test=\"journal-volume\">13<\/b>, 498\u2013503 (<span data-test=\"article-publication-year\">2020<\/span>)<\/a><\/p>\n<p>[4]:\u00a0 T. D\u00fcrig, F. Dioguardi, et al. A new method for the determination of the specific kinetic energy (SKE) released to pyroclastic particles at magmatic fragmentation: theory and first experimental results. Bulletin of Volcanology 74 (4) 895-902<\/p>\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Melt fragmentation experiments So, what has caused this abundance of ash during the 2012 Havre eruption? Let's draft a list of \"major suspects\", i.e. potential ash generation mechanisms that could have produced these fragments: Thermal granulation Magmatic fragmentation Fuel-coolant interaction &hellip; <a href=\"https:\/\/uni.hi.is\/tobi\/what-we-do-in-the-labs\/\">Continue reading <span class=\"meta-nav\">&rarr;<\/span><\/a><\/p>\n","protected":false},"author":1272,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"footnotes":""},"class_list":["post-1448","page","type-page","status-publish","hentry"],"_links":{"self":[{"href":"https:\/\/uni.hi.is\/tobi\/wp-json\/wp\/v2\/pages\/1448","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/uni.hi.is\/tobi\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/uni.hi.is\/tobi\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/uni.hi.is\/tobi\/wp-json\/wp\/v2\/users\/1272"}],"replies":[{"embeddable":true,"href":"https:\/\/uni.hi.is\/tobi\/wp-json\/wp\/v2\/comments?post=1448"}],"version-history":[{"count":12,"href":"https:\/\/uni.hi.is\/tobi\/wp-json\/wp\/v2\/pages\/1448\/revisions"}],"predecessor-version":[{"id":1634,"href":"https:\/\/uni.hi.is\/tobi\/wp-json\/wp\/v2\/pages\/1448\/revisions\/1634"}],"wp:attachment":[{"href":"https:\/\/uni.hi.is\/tobi\/wp-json\/wp\/v2\/media?parent=1448"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}